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CH40155: Advanced structural methods

Follow this link for further information on academic years Academic Year: 2012/3
Follow this link for further information on owning departmentsOwning Department/School: Department of Chemistry
Follow this link for further information on credits Credits: 3
Follow this link for further information on unit levels Level: Masters UG & PG (FHEQ level 7)
Follow this link for further information on period slots Period: Semester 1
Follow this link for further information on unit assessment Assessment: EX 100%
Follow this link for further information on supplementary assessment Supplementary Assessment: Like-for-like reassessment (where allowed by programme regulations)
Follow this link for further information on unit rules Requisites: Before taking this unit you must take CH20147 and in taking this unit you cannot take CH40131
Follow this link for further information on unit content Description: Aims:
To describe and give examples of some modern techniques for investigating the structure of a range of inorganic molecules.

Learning Outcomes:
After studying the Unit, students should be able to:
* Describe the physical basis, limitations and information available from structural methods, namely, X-Ray crystallography and NMR spectroscopy.
* Solve a range of problems by critically assessing numerical and spectroscopic information
* Solve problems using the techniques introduced including the application of techniques to unseen situations.

Skills:
Problem solving (T, F, A), Scientific writing (F, A), Independent working (F), Group working (F).

Content:
Brief introduction to crystallography. Crystal systems and lattices. Unit cells. Periodicity in lattices. Space group diagrams. Data collection procedures and solving crystal structures. Atomic scattering factors and structure factors. R factors.
Theoretical basis of NMR spectroscopy. Spin-spin coupling and chemical shifts in NMR spectroscopy and the factors that affect them. Spin systems.
First and second-order spectra. Isotopomers. NMR timescales and static and dynamic NMR spectra. Structural elucidation.
Follow this link for further information on programme availabilityProgramme availability:

CH40155 is Compulsory on the following programmes:

Department of Chemistry
  • USCH-AFM05 : MChem (hons) Chemistry for Drug Discovery (Full-time) - Year 4
  • USCH-AKM03 : MChem (hons) Chemistry for Drug Discovery with Industrial Training (Full-time with Thick Sandwich Placement) - Year 4
  • USCH-AAM06 : MChem (hons) Chemistry for Drug Discovery with Study Year Abroad (Full-time with Study Year Abroad) - Year 4

Notes:
* This unit catalogue is applicable for the 2012/13 academic year only. Students continuing their studies into 2013/14 and beyond should not assume that this unit will be available in future years in the format displayed here for 2012/13.
* Programmes and units are subject to change at any time, in accordance with normal University procedures.
* Availability of units will be subject to constraints such as staff availability, minimum and maximum group sizes, and timetabling factors as well as a student's ability to meet any pre-requisite rules.