Department of Chemistry, Unit Catalogue 2007/08 |
CH50100 Postgraduate training module |
| Credits: 6 |
| Level: Masters |
| Semester: 2 |
| Assessment: EX10%, CW 35%, OR15 %, OT 40% |
| Requisites: |
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Aims: The unit will provide training in three important techniques - X-ray crystallography, mass spectrometry and NMR spectroscopy - that are essential to the modern research chemist.
Learning Outcomes: After completing this unit, students should * have gained a basic understanding of crystallographic detail as reported in primary literature. * be familiar with CIF and RES file formats. * be competent with crystallographic display software that enables calculation of derived structural parameters from structural data files. * be able to generate publication quality molecular and lattice packing plots for crystal structures. * understand the importance of mass spectrometry as an analytical tool, along with an appreciation of the application areas where it is used. * be able to explain the basic operation mechanisms of several modern mass spectrometric analysers * be able to interpret a basic mass spectrum in positive and negative mode, including simple fragmentation patterns. * understand the principles of how pulsed NMR works, using the vector model. * understand common problems encountered in the day-to-day acquisition and processing of NMR spectra, how to solve them, and therefore how to achieve more satisfactory results. * have a knowledge of advanced NMR methods, with a focus on recently developed techniques. * present a talk focusing on the uses of one of these techniques. * communicate an understanding of the techniques to someone with the background understanding of a sixth form student. Skills: Data handling and analysis (T, F, A); Problem solving (T, F, A); Independent working (F); Oral communication (F): poster presentation (F). Content: 1 lecture per week on the techniques. 'Hands on' training and directed reading. Attendance at postgraduate seminars and Chemistry Department's series of general scientific lectures (the Millennium Lectures). Assessment will be by a combination of the following * multiple choice examination * data interpretation and manipulation assignments * a short oral presentation focusing on the uses of one of the techniques * a poster presentation. |